Benzoyl chloride → HCID 68123154, compound

HRID 328437Notes

Reaction equation

[CH3:1][N:2]([CH2:26][CH2:27][OH:28])[C:3](=[O:25])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14]/[CH:15]=[CH:16]\[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24].[C:29](Cl)(=[O:36])[C:30]1[CH:35]=[CH:34][CH:33]=[CH:32][CH:31]=1>>[CH3:1][N:2]([CH2:26][CH2:27][O:28][C:29](=[O:36])[C:30]1[CH:35]=[CH:34][CH:33]=[CH:32][CH:31]=1)[C:3](=[O:25])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14]/[CH:15]=[CH:16]\[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]

Participants

Reactant 2

HCID 7412Benzoyl chloride

HCID 86734640HCID 86734640, compound

Product 1

HCID 68123154HCID 68123154, compound

Procedure

N-methyl-N-(2-benzoyloxyethyl)erucamide was prepared by the procedure of example 1 from 39.5 gms. (0.1 mole) of N-methyl-N-(2-hydroxyethyl)erucamide and 14 gms. (0.1 mole) of benzoyl chloride. The structure of the final product was characterized on the basis of IR and NMR spectral analyses as described in example 1.

Workup

customN-methyl-N-(2-benzoyloxyethyl)erucamide was prepared by the procedure of example 1 from 39.5 gms

Sources & evidence

ORD record: ord-b0da95bfa1f647edb586bb8255659197
Source dataset: uspto-grants-1977_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04017522

Reaction notes

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