Benzoyl chloride → HCID 21441890, compound

HRID 328439Notes

Reaction equation

HRID 328439 reaction equation
[CH3:1][N:2]([CH2:20][CH2:21][OH:22])[C:3](=[O:19])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[C:23](Cl)(=[O:30])[C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1>>[CH3:1][N:2]([CH2:20][CH2:21][O:22][C:23](=[O:30])[C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1)[C:3](=[O:19])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]

Participants

3

Reactant 2

HCID 7412Benzoyl chlorideHCID 22321442N-(2-Hydroxyethyl)-N-methylhexadecanamide

Product 1

HCID 21441890HCID 21441890, compound

Procedure

N-methyl-N-(2-benzoyloxyethyl)palmitamide was prepared by the procedure of example 1 from 31 gms. (0.1 mole) of N-methyl-N-(2-hydroxyethyl)palmitamide and 14 gms. (0.1 mole) of benzoyl chloride. The structure of the final product was characterized on the basis of IR and NMR spectral analyses as described in example 1.

Workup

  1. customN-methyl-N-(2-benzoyloxyethyl)palmitamide was prepared by the procedure of example 1 from 31 gms

Sources & evidence

ORD record
ord-616713b3807f44b3ae1bc7816e037ef4
Source dataset
uspto-grants-1977_04
Patent number
US04017522

Reaction notes

Loading…