2-Furancarbonyl chloride → HCID 54339264, compound

HRID 328440Notes

Reaction equation

HRID 328440 reaction equation
[CH3:1][N:2]([CH2:20][CH2:21][OH:22])[C:3](=[O:19])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[O:23]1[CH:27]=[CH:26][CH:25]=[C:24]1[C:28](Cl)=[O:29]>>[CH3:1][N:2]([CH2:20][CH2:21][O:22][C:28]([C:24]1[O:23][CH:27]=[CH:26][CH:25]=1)=[O:29])[C:3](=[O:19])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]

Participants

3

Reactant 2

HCID 682422-Furancarbonyl chlorideHCID 22321442N-(2-Hydroxyethyl)-N-methylhexadecanamide

Product 1

HCID 54339264HCID 54339264, compound

Procedure

N-methyl-N-(2-furoyloxyethyl)palmitamide was prepared by the procedure of example 1 from 31 gms. (0.1 mole) of N-methyl-N-(2-hydroxyethyl)palmitamide and 13 gms. (0.1 mole) of furoyl chloride. The structure of the final product was characterized on the basis of IR and NMR spectral analyses as described in example 1.

Workup

  1. customN-methyl-N-(2-furoyloxyethyl)palmitamide was prepared by the procedure of example 1 from 31 gms

Sources & evidence

ORD record
ord-4f6e92ee1c7e4e88a9e9fc5ed3326f38
Source dataset
uspto-grants-1977_04
Patent number
US04017522

Reaction notes

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