Dodecanoyl chloride → 2-[Methyl(4-methylbenzoyl)amino]ethyl dodecanoate

HRID 328443Notes

Reaction equation

HRID 328443 reaction equation
[CH3:1][N:2]([CH2:12][CH2:13][OH:14])[C:3]([C:5]1[CH:10]=[CH:9][C:8]([CH3:11])=[CH:7][CH:6]=1)=[O:4].[C:15](Cl)(=[O:27])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26]>>[CH3:1][N:2]([CH2:12][CH2:13][O:14][C:15](=[O:27])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26])[C:3]([C:5]1[CH:10]=[CH:9][C:8]([CH3:11])=[CH:7][CH:6]=1)=[O:4]

Participants

3

Reactant 2

HCID 8166Dodecanoyl chlorideHCID 21441887N-(2-hydroxyethyl)-N,4-dimethylbenzamide

Product 1

HCID 214418812-[Methyl(4-methylbenzoyl)amino]ethyl dodecanoate

Procedure

N-methyl-N-(2-lauroyloxyethyl)-p-toluamide was prepared by the procedure of example 1 from 19 gms. (0.1 mole) of N-methyl-N-(2-hydroxyethyl)-p-toluamide and 22 gms. (0.1 mole) of lauroyl chloride. The structure of the final product was characterized on the basis of IR and NMR spectral analyses as described in example 1.

Workup

  1. customN-methyl-N-(2-lauroyloxyethyl)-p-toluamide was prepared by the procedure of example 1 from 19 gms

Sources & evidence

ORD record
ord-18cfc6ff3a2249b884f95b49c1629176
Source dataset
uspto-grants-1977_04
Patent number
US04017522

Reaction notes

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