HRID328460

反应详情

EQUATION

反应方程式

HRID 328460 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a mixture of 22.1 g of acetyl cyanide and 16.3 g of diaminomaleonitrile were added dropwise a solution of 0.5 g of phosphorus pentoxide in 3 ml of methanol. The crude product thus obtained was recrystallized from aqueous methanol to obtain 6.3 g (26% yield) of α-cyanoethylidenediaminomaleonitrile.

WORKUP

后处理

  1. customThe crude product thus obtained
  2. customwas recrystallized from aqueous methanol