HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Isocyanate → HCID 178485944, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | HCID 140604579 | HCID 140604579 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178485944 | HCID 178485944 | — |
Reaction Steps
A mixture of 13 parts of methyl thioallophanimidate 74 parts of methylene chloride and 6 parts of methylisocyanate is refluxed for 2 hours. After standing overnight at room temperature, the solution is evaporated under vacuum to give crude methyl N-carbamoyl-4-methylthioallophanimidate (a compound of formula I).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04017529 |
| Source dataset | uspto-grants-1977_04 |
| ORD ID | ord-f02c9cd9fff94cc0909c3a74bfd1250a |
| Source note | uspto-grants-1977_04 |