HCID 12760617, compound → HCID 86734655, compound

HRID 328647Notes

Reaction equation

HRID 328647 reaction equation
[CH2:1]([O:5][CH:6]([C:13]1[CH:18]=[CH:17][C:16]([Cl:19])=[CH:15][C:14]=1[Cl:20])[CH2:7][N:8]1[CH:12]=[CH:11][N:10]=[CH:9]1)[CH2:2][CH2:3][CH3:4].[Cl:21][C:22]1[CH:27]=[CH:26][C:25]([CH:28](Cl)[C:29]2[CH:34]=[CH:33][C:32]([F:35])=[CH:31][CH:30]=2)=[CH:24][CH:23]=1>C(#N)C>[Cl-:19].[CH2:1]([O:5][CH:6]([C:13]1[CH:18]=[CH:17][C:16]([Cl:19])=[CH:15][C:14]=1[Cl:20])[CH2:7][N+:8]1[CH:12]=[CH:11][N:10]([CH:28]([C:29]2[CH:34]=[CH:33][C:32]([F:35])=[CH:31][CH:30]=2)[C:25]2[CH:24]=[CH:23][C:22]([Cl:21])=[CH:27][CH:26]=2)[CH:9]=1)[CH2:2][CH2:3][CH3:4]

Participants

4

Reactant 2

HCID 12760617HCID 12760617, compoundHCID 21730336HCID 21730336, compound

Product 1

HCID 86734655HCID 86734655, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

6.3 Parts of 1-(β-butoxy-2,4-dichlorophenethyl)-imidazole and 5.1 parts of (p-chlorophenyl) (p-fluorophenyl)methyl chloride are mixed together in 80 parts of acetonitrile and the resulting mixture is stirred at reflux temperature overnight. Thereafter, the solvent is vaporized off to obtain as residue a 1-(β-butoxy-2,4-dichlorophenethyl)-3-[p-chloro-α-(p-fluorophenyl)benzyl]imidazolium chloride product.

Workup

  1. temperatureat reflux temperature overnight

Sources & evidence

ORD record
ord-638ed155ba784c3493432540d5c87a0f
Source dataset
uspto-grants-1977_04
Patent number
US04017631

Reaction notes

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