HRID328747

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID241

Benzene

C6H6

HCID6386

tert-Butyl alcohol

C4H10O

结构：O=C(Cl)c1ccc([N+](=O)[O-])c([N+](=O)[O-])c1

HCID11806491

3,4-dinitrobenzoyl Chloride

C7H3ClN2O5

PRODUCTS

生成物

结构：CC(C)(C)OC(=O)c1ccc([N+](=O)[O-])c([N+](=O)[O-])c1

HCID20551560

tert-Butyl 3,4-dinitrobenzoate

C11H12N2O6

收率 49%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID1049

Pyridine

C5H5N

PROCEDURE

实验过程

The crude 3,4-dinitrobenzoyl chloride, 500 ml. of benzene, 25 ml. of pyridine and 22 g. (0.3 mole) of t-butyl alcohol were reacted as in Example 2 (A), second paragraph, to provide 33 g. (49 percent yield) of t-butyl 3,4-dinitrobenzoate.

WORKUP

后处理

customto provide 33 g