HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanogen Bromide → HCID 21317655, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanogen Bromide | HCID 10476 | — |
| Reactant | HCID 21317579 | HCID 21317579 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 21317655 | HCID 21317655 | — |
Reaction Steps
A solution of cyanogen bromide (36.0 g., 0.340 mole) in ether (400 ml.) is treated with 1-diethylamino-4-acetoxy-5,5-dimethyl-2-nonyne (82.3 g., 0.293 mole) to give a mildly exothermic reaction. The clear solution is allowed to stand at room temperature for 16 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04018802 |
| Source dataset | uspto-grants-1977_04 |
| ORD ID | ord-2e0f29ab189c4e3fb6a9e4e291587c3c |
| Source note | uspto-grants-1977_04 |