HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 22757891, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Phosphinecarboxylic acid, 1,1-diethoxy-, ethyl ester, 1-oxide | HCID 65081 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 22757891 | HCID 22757891 | — |
Reaction Steps
Using the method of Nylen, Ber., 57B, 1023 (1924), a solution of 21 parts of triethyl carboxyphosphonate in 60 parts of water containing 24 parts of 50% sodium hydroxide was refluxed for 2 hrs. The solution was allowed to cool overnight. Filtration of the reaction mixture gave 4.7 parts of the product, trisodium carboxyphosphonate hexahydrate, mp >250°; νKBr = 1560, 1530 cm-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04018854 |
| Source dataset | uspto-grants-1977_04 |
| ORD ID | ord-8b2519762ae2408b9950465ac5162358 |
| Source note | uspto-grants-1977_04 |