HCID 21440130, compound → HCID 12408785, compound

HRID 328935Notes

Reaction equation

HRID 328935 reaction equation
[C:1]([C:9]1[C:17]([N+:18]([O-])=O)=[CH:16][C:12]([C:13]([OH:15])=[O:14])=[CH:11][C:10]=1[O:21][CH2:22][CH2:23][CH2:24]C)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C(C1C([N+]([O-])=O)=CC(C(O)=O)=CC=1OCCC)(=O)C1C=CC=CC=1>>[NH2:18][C:17]1[C:9]([C:1](=[O:8])[C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)=[C:10]([O:21][CH2:22][CH2:23][CH3:24])[CH:11]=[C:12]([CH:16]=1)[C:13]([OH:15])=[O:14]

Participants

3

Reactant 2

HCID 21440130HCID 21440130, compoundHCID 21440215HCID 21440215, compound

Product 1

HCID 12408785HCID 12408785, compound

Procedure

By replacing in Example 1, step C, 4-benzoyl-3-n-butoxy-5-nitrobenzoic acid with 4-benzoyl-5-nitro-3-n-propoxybenzoic acid and following the procedure described, 5-amino-4-benzoyl-3-n-propoxybenzoic acid is obtained with a melting point of 220° -222° C.

Sources & evidence

ORD record
ord-58ddebd98db7456e99bbb9b2a32460c3
Source dataset
uspto-grants-1977_04
Patent number
US04018794

Reaction notes

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