HCID 21440223, compound → HCID 178507794, compound

HRID 328963Notes

Reaction equation

HRID 328963 reaction equation
C(C1C([N+]([O-])=O)=CC(C(O)=O)=CC=1OCC1C=CC=CC=1)(=O)C1C=CC=CC=1.[NH2:29][C:30]1[C:31]([C:46](=O)[C:47]2[CH:52]=[CH:51][CH:50]=[CH:49][CH:48]=2)=[C:32]([CH2:39][C:40]2[CH:45]=[CH:44][CH:43]=[CH:42][CH:41]=2)[CH:33]=[C:34]([CH:38]=1)[C:35]([OH:37])=[S:36]>>[NH2:29][C:30]1[C:31]([CH2:46][C:47]2[CH:52]=[CH:51][CH:50]=[CH:49][CH:48]=2)=[C:32]([CH2:39][C:40]2[CH:45]=[CH:44][CH:43]=[CH:42][CH:41]=2)[CH:33]=[C:34]([CH:38]=1)[C:35]([OH:37])=[S:36]

Participants

3

Reactant 2

HCID 21440223HCID 21440223, compoundHCID 178507795HCID 178507795, compound

Product 1

HCID 178507794HCID 178507794, compound

Procedure

By replacing in Example 24, step A, 4-benzoyl-3-benzyloxy-5-nitrobenzoic acid with 5-amino-4-benzoyl-3-benzylthiobenzoic acid and following the procedure described, 5-amino-4-benzyl-3-benzylthiobenzoic acid is obtained with a melting point of 256°-257° C.

Sources & evidence

ORD record
ord-0f44aee317194c94994a4590bb861240
Source dataset
uspto-grants-1977_04
Patent number
US04018794

Reaction notes

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