HCID 21440140, compound → HCID 21440192, compound

HRID 328972Notes

Reaction equation

HRID 328972 reaction equation
[CH2:1](C1C(S(=O)(=O)N)=CC(C(O)=O)=CC=1SCCCC)C1C=CC=CC=1.[CH2:26]([C:33]1[C:41]([S:42](=[O:45])(=[O:44])[NH2:43])=[CH:40][C:36]([C:37]([OH:39])=[O:38])=[CH:35][C:34]=1[S:46][CH2:47][C:48]1[CH:53]=[CH:52][CH:51]=[CH:50][CH:49]=1)[C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1>>[CH2:26]([C:33]1[C:41]([S:42](=[O:45])(=[O:44])[NH2:43])=[CH:40][C:36]([C:37]([O:39][CH3:1])=[O:38])=[CH:35][C:34]=1[S:46][CH2:47][C:48]1[CH:53]=[CH:52][CH:51]=[CH:50][CH:49]=1)[C:27]1[CH:28]=[CH:29][CH:30]=[CH:31][CH:32]=1

Participants

3

Reactant 2

HCID 21440140HCID 21440140, compoundHCID 54516912HCID 54516912, compound

Product 1

HCID 21440192HCID 21440192, compound

Procedure

By replacing in Example 124, 4-benzyl-3-n-butylthio-5-sulfamylbenzoic acid with 4-benzyl-3-benzylthio-5-sulfamylbenzoic acid and following the procedure described, methyl 4-benzyl-3-benzylthio-5-sulfamylbenzoate is obtained with a melting point of 139°-140° C.

Sources & evidence

ORD record
ord-662bca545e494cbebcd92d25da481d19
Source dataset
uspto-grants-1977_04
Patent number
US04018794

Reaction notes

Loading…