HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 178486632, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 178486646 | HCID 178486646 | — |
| Product | HCID 178486632 | HCID 178486632 | — |
Reaction Steps
A suspension of 2.00 g of N2 -(6,7-dimethoxy-2-naphthalenesulfonyl)-L-arginine in 20 ml of thionyl chloride was stirred for 2 hours at room temperature. Addition of cold dry diethyl ether resulted in a precipitate which was collected by filtration and washed several times with dry diethyl ether to give N2 -(6,7-dimethoxy-2-naphthalenesulfonyl)-L-arginyl chloride hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04018915 |
| Source dataset | uspto-grants-1977_04 |
| ORD ID | ord-d756bfff1dba4bf6bd7055bf0b8daddd |
| Source note | uspto-grants-1977_04 |