HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Aminopyridazine-3-carboxylic acid → (6-Aminopyridazin-3-yl)methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Aminopyridazine-3-carboxylic acid | HCID 12200479 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | (6-Aminopyridazin-3-yl)methanol | HCID 20557894 | — |
Reaction Steps
6-Amino-3-pyridazinecarboxylic acid is converted to the methyl ester and the ester is reduced with lithium aluminium hydride in tetrahydrofuran to give 6-amino-3-hydroxymethylpyridazine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04018931 |
| Source dataset | uspto-grants-1977_04 |
| ORD ID | ord-0e0f90a3a96e47d2a253352083cb5e50 |
| Source note | uspto-grants-1977_04 |