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HRID329087

反应详情

EQUATION

反应方程式

HRID 329087 的结构方程式

REACTANTS

反应物

2
结构：CN(C)CCN=C=S
HCID3853726

2-Isothiocyanato-N,N-dimethylethan-1-amine

C5H10N2S

结构：NCCNCc1ncccn1
HCID20557649

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)CCNC(=S)NCCNCc1ncccn1
HCID20557883

未命名化合物

PROCEDURE

实验过程

Treating N-(2-pyrimidylmethyl)ethylenediamine with 2-dimethylaminoethyl isothiocyanate, then concentrating and separating by column chromatography by the procedure of Example 40 (a)(ii) gives the title compound.

WORKUP

后处理

  1. concentrationconcentrating
  2. customseparating by column chromatography by the procedure of Example 40 (a)(ii)