HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium → 2-{[1-(4-Chlorophenyl)ethyl]sulfanyl}-1-oxo-1lambda~5~-pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 1-chloro-4-(1-chloroethyl)benzene | HCID 10975999 | — |
| Reactant | HCID 178526253 | HCID 178526253 | — |
| Product | 2-{[1-(4-Chlorophenyl)ethyl]sulfanyl}-1-oxo-1lambda~5~-pyridine | HCID 54133270 | 78% |
Reaction Steps
The intermediate 2-(1-[4-chlorophenyl]ethylthio)-pyridine N-oxide is prepared from 1-(4-chlorophenyl)ethylchloride and 2-mercaptopyridine N-oxide, sodium salt by the procedure described in Example 2. Melting point 106° - 108° C. Structure confirmed by IR and NMR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04019893 |
| Source dataset | uspto-grants-1977_04 |
| ORD ID | ord-a7071554eda24f05b2de93a1ef72eeed |
| Source note | uspto-grants-1977_04 |