HRID329146

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID11093

1-(Chloromethyl)-2-methylbenzene

C8H9Cl

HCID178507102

未命名化合物

PRODUCTS

生成物

HCID45692352

2-{[(2-Methylphenyl)methyl]sulfanyl}-1-oxo-1lambda~5~-pyridine

C13H13NOS

收率 85%

PROCEDURE

实验过程

The intermediate 2-(2-methylphenylmethylthio)pyridine N-oxide is prepared by the procedure described in Example 2 from α-chloro o-xylene and 2-mercaptopyridine N-oxide sodium salt. Melting point 134° -136° C. Yield 85% theory. Structure confirmed by IR and NMR.