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1-Bromo-4-(1-chloroethyl)benzene → 2-{[1-(4-Bromophenyl)ethyl]sulfanyl}-1-oxo-1lambda~5~-pyridine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Bromo-4-(1-chloroethyl)benzene | HCID 14557467 | — |
| 反応物 | HCID 178507102 | HCID 178507102 | — |
| 生成物 | 2-{[1-(4-Bromophenyl)ethyl]sulfanyl}-1-oxo-1lambda~5~-pyridine | HCID 54500435 | 85% |
反応手順
The compound 2-(1-[4-bromophenyl]ethylthio)pyridine N-oxide is prepared from 1-(4-bromophenyl)ethylchloride and 2-mercaptopyridine N-oxide sodium salt by the procedure described in Example 1. The melting point is 113° - 115° C. Structure is confirmed by IR and NMR.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04019893 |
| 出典データセット | uspto-grants-1977_04 |
| ORD ID | ord-32d52c5bcd5846b6ab79f4a6c630f3c8 |
| 出典メモ | uspto-grants-1977_04 |