HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Alcohol → HCID 12261647, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Alcohol | HCID 244 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ethyl isothiocyanatoformate | HCID 85320 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 12261647 | HCID 12261647 | 71.6% |
Reaction Steps
A mixture of 162 g of benzyl alcohol and 196 g of ethoxycarbonyl isothiocyanate and 1 ml of triethylamine in 1 liter of tetrahydrofuran was refluxed for 24 hours and was concentrated to dryness. The residue was washed with petroleum ether and isopropyl ether to obtain 256 g of benzyl N-carbethoxy-thiocarbamate melting at 96° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04020076 |
| Source dataset | uspto-grants-1977_04 |
| ORD ID | ord-63d88ebacf7145f5aff281b3714eba4f |
| Source note | uspto-grants-1977_04 |