O-Phenylenediamine → HCID 21538751, compound

HRID 329219Notes

Reaction equation

HRID 329219 reaction equation
[C:1]1([NH2:8])[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[NH2:7].[Cl:9][C:10]1[CH:21]=[CH:20][C:13]([O:14][C:15]([N:17]=[C:18]=[S:19])=[O:16])=[CH:12][CH:11]=1>>[Cl:9][C:10]1[CH:21]=[CH:20][C:13]([O:14][C:15]([NH:17][C:18](=[S:19])[NH:7][C:2]2[CH:3]=[CH:4][CH:5]=[CH:6][C:1]=2[NH:8][C:18]([NH:17][C:15]([O:14][C:13]2[CH:20]=[CH:21][C:10]([Cl:9])=[CH:11][CH:12]=2)=[O:16])=[S:19])=[O:16])=[CH:12][CH:11]=1

Participants

3

Reactant 2

HCID 7243O-PhenylenediamineHCID 13160296HCID 13160296, compound

Product 1

HCID 21538751HCID 21538751, compound

Procedure

3.3 g. of o-phenylenediamine were dropped into the mixture containing the resulting 4-chlorophenoxycarbonylisothiocyanate at a temperature of 0°-20° C.

Sources & evidence

ORD record
ord-11df9b6e59be4aa386dbb4ab2517eb56
Source dataset
uspto-grants-1977_04
Patent number
US04020095

Reaction notes

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