4-Methoxyphenol → HCID 22759317, compound
Reaction equation
[CH3:1][O:2]C1C=CC(O)=CC=1.[C:10]([CH:13]([CH2:23][CH2:24][CH2:25][CH:26]([OH:39])[CH2:27][O:28][C:29]1[CH:34]=[CH:33][C:32](C(C)(C)C)=[CH:31][CH:30]=1)[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][C:20]([OH:22])=[O:21])(=[O:12])[CH3:11]>>[C:10]([CH:13]([CH2:23][CH2:24][CH2:25][CH:26]([OH:39])[CH2:27][O:28][C:29]1[CH:30]=[CH:31][C:32]([O:2][CH3:1])=[CH:33][CH:34]=1)[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][C:20]([OH:22])=[O:21])(=[O:12])[CH3:11]Participants
3
Procedure
The synthesis of this compound is carried out by the procedure of Example 10 except that an equivalent amount of 4-methoxyphenol is substituted for the 4-tert-butylphenol of Example 10. The title compound is obtained as a viscous oil after purification by silica gel column chromatography.
Workup
- customThe synthesis of this compound
Sources & evidence
- ORD record
- ord-5b29c905f6104204abd133f1fbd5cc4c
- Source dataset
- uspto-grants-1977_04
- Patent number
- US04020177
Reaction notes
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