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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 329331Generated: October 28, 2026

Diethylethanolamine → beta-N-N-diethylaminoethyl-2-(5-oxo-5H-dibenzo[a,d]cyclohepten-2-yl)propionate

https://huagongshe.com/reaction/329331

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiethylethanolamineHCID 7497—
ReactantN-Ethyl-N-methylethanolamineHCID 17916—
ReactantHCID 12398827HCID 12398827—
Productbeta-N-N-diethylaminoethyl-2-(5-oxo-5H-dibenzo[a,d]cyclohepten-2-yl)propionateHCID 12398842—

Reaction Steps

In similar manner substituting diethylethanolamine and N-ethyl-N-methylethanolamine for the dimethylethanolamine, there is obtained β-N-N-diethylaminoethyl-2-(5-oxo-5H-dibenzo[a,d]cyclohepten-2-yl)propionate as an oil (hydrochloride salt: m.p. 117°-123° C; see Example XIV) and β-N-ethyl-N-methylaminoethyl 2-(5-oxo-5H-dibenzo[a,d]cyclohepten-2-yl)-propionate [an oil; n.m.r. spectrum in deuterochloroform relative to tetramethylsilane: 0.94 (triplet, CH2CH3); 1.53 (doublet, CHCH3); 2.08 (singlet, N--CH3); 4.17 (triplet, OCH2) and 7.03 ppm (singlet, 10H,11H); mass spectrum: 363 (M+), 305, 233, 205].

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04020094
Source datasetuspto-grants-1977_04
ORD IDord-539ff5670e564f4286e8b1c3c4675632
Source noteuspto-grants-1977_04