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HRID329432

反应详情

EQUATION

反应方程式

HRID 329432 的结构方程式

REACTANTS

反应物

3
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CO
HCID887

Methanol

CH4O

结构：CC(=O)Oc1cc(C(=O)O)c(C(=O)NC(C)(C(N)=O)C(C)C)nc1C
HCID13799445

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)c1cc(OC(C)=O)c(C)nc1C(=O)NC(C)(C(N)=O)C(C)C
HCID13799446

未命名化合物

PROCEDURE

实验过程

Hydrochloric acid gas is led for 3 hours through a solution of 53 g (0.151 mol) 5-acetoxy-2-(1-carbamoyl-1,2-dimethylpropyl-carbamoyl)-6-methyl-nicotinic acid in 500 ml absolute methanol boiling under reflux. Then, the solvent is evaporated and the product is dried in a vacuum.

WORKUP

后处理

  1. temperatureunder reflux
  2. customThen, the solvent is evaporated
  3. customthe product is dried in a vacuum