HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → 4,4'-Dihydroxybiphenyl
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Product | 4,4'-Dihydroxybiphenyl | HCID 7112 | 91% |
Reaction Steps
The procedures of Example 12 were repeated except that 10.0 g of reaction solution (1) obtained in Example 12, 0.1 g of phenol (solvent) and 0.04 g of sulfuric acid (catalyst) were added to the whole portion of mother liquor (I) obtained in Example 12 and that reaction was performed at 185° C. for 3 hours to produce p,p'-biphenol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04891453 |
| Source dataset | uspto-grants-1990_01 |
| ORD ID | ord-c0d019008bb540f8b2221145f258ff91 |
| Source note | uspto-grants-1990_01 |