HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → 2-Chloro-4-methylamino-6-amino-1,3,5-triazine-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 4,6-Dichloro-1,3,5-trazin-2-amine | HCID 13615 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 2-Chloro-4-methylamino-6-amino-1,3,5-triazine- | HCID 224970 | — |
Reaction Steps
A solution of 2-amino-4,6-dichloro-1,3,5-triazine (0.2 mole) in 200 ml reagent grade acetone was cooled to 0° C. Two equivalents of 40% aqueous methylamine were added dropwise keeping the temperature less than 10° C.; solids precipitated during the addition. The reaction was then warmed to room temperature and stirred overnight under N2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04892575 |
| Source dataset | uspto-grants-1990_01 |
| ORD ID | ord-436970b16920477c90f335b3826c7607 |
| Source note | uspto-grants-1990_01 |