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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 329590Generated: October 25, 2026

17beta-Acetoxy-1alpha-methyl-17alpha-n-propyl-5alpha-androstan-3-one → 17beta-Acetoxy-1alpha-methyl-17alpha-n-propyl-5alpha-androstan-3beta-ol

https://huagongshe.com/reaction/329590

Reaction equation

Participants

RoleNameHCIDCharge
Reactant17beta-Acetoxy-1alpha-methyl-17alpha-n-propyl-5alpha-androstan-3-oneHCID 13020886—
ReactantLithium tri-tert-butoxyaluminohydrideHCID 16710494—
Product17beta-Acetoxy-1alpha-methyl-17alpha-n-propyl-5alpha-androstan-3beta-olHCID 7036026164.7%

Reaction Steps

1.0 g of 17β-acetoxy-1α-methyl-17α-n-propyl-5α-androstan-3-one is reacted as described in Example 6 with lithium tri-tert.-butoxyaluminum hydride and worked up. After chromatography on silica gel, 650 mg of 17β-acetoxy-1α-methyl-17α-n-propyl-5α-androstan-3β-ol is obtained as an oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04892867
Source datasetuspto-grants-1990_01
ORD IDord-adeedd16207e4916ba3804d85c5050fb
Source noteuspto-grants-1990_01