HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 15595654, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 6-(m-Acetamidophenyl)-1,2,4-triazolo[4,3-b]pyridazine | HCID 7532146 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 15595654 | HCID 15595654 | — |
Reaction Steps
A mixture of 1.82 g of N-[3-(1,2,4-triazolo[4,3-b]pyridazin-6-yl)phenyl]acetamide, 0.43 g of sodium hydride (50% in oil), 100 ml of dimethylformamide and 0.7 ml of ethyl iodide were reacted as described in Example 9, giving 1.20 g of the desired product as tan crystals mp 122°-127° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04892873 |
| Source dataset | uspto-grants-1990_01 |
| ORD ID | ord-8fd808397fe840d780b37d5cbe9f07e8 |
| Source note | uspto-grants-1990_01 |