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HRID329655

反应详情

EQUATION

反应方程式

HRID 329655 的结构方程式

REACTANTS

反应物

2
结构：CN(C)Cc1ccccc1P(c1ccccc1)c1ccccc1
HCID11370610

未命名化合物

结构：COC(=O)N=[N+]=[N-]
HCID12542276

Methyl carbonazidate

C2H3N3O2

PRODUCTS

生成物

1
结构：COC(=O)N=P(c1ccccc1)(c1ccccc1)c1ccccc1CN(C)C
HCID14771585

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOCC
溶剂HCID3283

Diethyl Ether

C4H10O

PROCEDURE

实验过程

A 2.0 g portion of 2-(diphenylphosphino)-N,N-dimethylbenzenemethanamine was reacted with 4.0 ml of 1M methyl carbonazidate in ether as described in Example 1, giving 1.32 g of the desired product, mp 95°-97° C.