HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzyl Bromide → 1-(Phenylmethyl)pyrrolidine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzyl Bromide | HCID 7498 | — |
| Edukt | Pyrrolidine | HCID 31268 | — |
| Lösungsmittel | Diethyl Ether | HCID 3283 | — |
| Produkt | 1-(Phenylmethyl)pyrrolidine | HCID 122501 | — |
Reaktionsschritte
A 25.0 ml portion of pyrrolidine was reacted with 10.9 ml of benzyl bromide in ether as described in Example 3, giving 12.3 g of 1-(phenylmethyl)pyrrolidine, which was then reacted with butyl lithium and diphenylphosphine chloride as described in Example 3, giving diphenyl]2-(1-pyrrolidinylmethyl)phenyl]phosphine.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04892885 |
| Quelldatensatz | uspto-grants-1990_01 |
| ORD ID | ord-9293d2e303a2441eba00c7ae2796c964 |
| Quellennotiz | uspto-grants-1990_01 |