HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 329699Generated: October 26, 2026
1,1,3,3-Tetramethyl-disiloxane → 1,3-bis(N-cyclohexyl-3-aminopropyl)-1,1,3,3-tetramethyldisiloxane
https://huagongshe.com/reaction/329699
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1,1,3,3-Tetramethyl-disiloxane | HCID 18659 | — |
| Reactant | N-Allylcyclohexylamine | HCID 81115 | — |
| Catalyst | Chloroplatinic acid | HCID 61859 | — |
| Product | 1,3-bis(N-cyclohexyl-3-aminopropyl)-1,1,3,3-tetramethyldisiloxane | HCID 19871404 | — |
Reaction Steps
Following the technique described in Example 1, N-allylcyclohexylamine (0.173 mole), 1,1,3,3-tetramethyldisiloxane (0.0783 mole), and 0.05 g hexachloroplatinic acid are stirred at 70° C for eight hours at 110° C. under nitrogen. The product, in nearly quantitative yield, is purified by vacuum distillation at <1 torr at a temperature of 207°-210° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04892918 |
|---|
| Source dataset | uspto-grants-1990_01 |
|---|
| ORD ID | ord-c0289677df37416ba173f315dea44ca7 |
|---|
| Source note | uspto-grants-1990_01 |
|---|
