2-Amino-4-methoxy-6-methyl-1,3,5-triazine → HCID 19871586, compound

HRID 329758Notes

Reaction equation

HRID 329758 reaction equation
[CH3:1][O:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([N:11]=[C:12]=[O:13])=[CH:7][C:6]=1[S:14]([N:17]=[C:18]=[O:19])(=[O:16])=[O:15])=[O:4].[NH2:20][C:21]1[N:26]=[C:25]([O:27][CH3:28])[N:24]=[C:23]([CH3:29])[N:22]=1>C(#N)C>[CH3:1][O:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([N:11]=[C:12]=[O:13])=[CH:7][C:6]=1[S:14]([NH:17][C:18]([NH:20][C:21]1[N:26]=[C:25]([O:27][CH3:28])[N:24]=[C:23]([CH3:29])[N:22]=1)=[O:19])(=[O:15])=[O:16])=[O:4]

Participants

4

Reactant 2

HCID 154662-Amino-4-methoxy-6-methyl-1,3,5-triazineHCID 19871572HCID 19871572, compound

Product 1

HCID 19871586HCID 19871586, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

To 27 g of 2-methoxycarbonyl-5-isocyanatobenzenesulfonylisocyanate in 250 ml of anhydrous acetonitrile is added in small portions at ambient temperatures, 14 g of 2-amino-4-methoxy-6-methyl-1,3,5-triazine, the mixture is then stirred at ambient temperature for 16 hours. The resultant product, a white precipitate is removed by filtration and dried in vacuo.

Workup

  1. customThe resultant product, a white precipitate is removed by filtration
  2. customdried in vacuo

Sources & evidence

ORD record
ord-0b5e0fe9526348c9900e76a584662da3
Source dataset
uspto-grants-1990_01
Patent number
US04892946

Reaction notes

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