HCID 19871645, compound → HCID 67933355, compound

HRID 329781Notes

Reaction equation

HRID 329781 reaction equation
[CH3:1][C:2]([C:5]1[CH:10]=[CH:9][C:8]([N:11]([CH3:20])[C:12]([C:14]2[CH:15]=[N:16][O:17][C:18]=2[CH3:19])=[O:13])=[CH:7][CH:6]=1)([CH3:4])[CH3:3]>C(O)C.[OH-].[K+]>[C:15]([C:14](=[C:18]([OH:17])[CH3:19])[C:12]([N:11]([C:8]1[CH:7]=[CH:6][C:5]([C:2]([CH3:1])([CH3:4])[CH3:3])=[CH:10][CH:9]=1)[CH3:20])=[O:13])#[N:16]

Participants

4

Reactant 1

HCID 19871645HCID 19871645, compound

Product 1

HCID 67933355HCID 67933355, compound

Reagents, catalysts & solvents 2

HCID 702EthanolSolventHCID 14797Potassium HydroxideSolvent

Procedure

N-[4-(1,1-Dimethylethyl)phenyl]-N-methyl-5-methylisoxazol-4-ylcarboxamide (9.8 g) was magnetically stirred in absolute ethanol (200 ml) and 1N potassium hydroxide solution (36 ml). Within 10 minutes a clear solution had resulted.

Workup

  1. customWithin 10 minutes a clear solution had resulted

Sources & evidence

ORD record
ord-53702e1729444cf4b09e5ebbb3b23aff
Source dataset
uspto-grants-1990_01
Patent number
US04892963

Reaction notes

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