1-(1-methylcyclopropyl)-4-nitrobenzene → HCID 7048506, compound

HRID 329783Notes

Reaction equation

HRID 329783 reaction equation
[CH3:1][C:2]1([C:5]2[CH:10]=[CH:9][C:8]([NH:11][C:12]([C:14]3[CH:15]=[N:16][O:17][C:18]=3[CH3:19])=[O:13])=[CH:7][CH:6]=2)[CH2:4][CH2:3]1.NC1C=CC(C2(C)CC2)=CC=1.CC1(C2C=CC([N+]([O-])=O)=CC=2)CC1>>[CH3:4][C:2]([C:5]1[CH:6]=[CH:7][C:8]([NH:11][C:12]([C:14]2[CH:15]=[N:16][O:17][C:18]=2[CH3:19])=[O:13])=[CH:9][CH:10]=1)([CH3:1])[CH3:3]

Participants

4

Reactant 3

HCID 15183601-(1-methylcyclopropyl)-4-nitrobenzeneHCID 19871647HCID 19871647, compoundHCID 19871650HCID 19871650, compound

Product 1

HCID 7048506HCID 7048506, compound

Procedure

N-[4-(1-methylcyclopropyl)phenyl]-5-methylisoxazol-4-yl-carboxamide, viscous oil (from 1-amino-4-(1-methylcyclopropyl)benzene, b.p. 65°-70° C./0.25 mm Hg, prepared by reduction of 1-(1-methylcyclopropyl)-4-nitrobenzene, Chem.Ber. 106 525-548 (1973)).

Sources & evidence

ORD record
ord-77f3fa37ddda4748b88174a7337366fa
Source dataset
uspto-grants-1990_01
Patent number
US04892963

Reaction notes

Loading…