HCID 19871542, compound → 1-Methylpyridin-1-ium acetate

HRID 329826Notes

Reaction equation

HRID 329826 reaction equation
C[O:2][C:3](=[O:5])[O-].[CH3:6][N+:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1>C(O)(=O)C>[C:3]([O-:2])(=[O:5])[CH3:6].[CH3:6][N+:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1

Participants

3

Reactant 1

HCID 19871542HCID 19871542, compound

Product 1

HCID 234472881-Methylpyridin-1-ium acetateYield 192.2%

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

By following the same procedure as Example 6 except that 10.0 g of N-methylpyridinium methyl carbonate obtained in the 1st step of Example 4 and 3.1 g of acetic acid were used, 8.7 g (yield of 75.4% of pyridine) of N-methylpyridinium acetate was obtained.

Sources & evidence

ORD record
ord-fc3f6f174e63439db2910e0cd9b52acd
Source dataset
uspto-grants-1990_01
Patent number
US04892944

Reaction notes

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