HuagongsheHuagongshe Chemistry Print Report · For research reference only
Perchlorate → Phenylphosphine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Perchlorate | HCID 123351 | — |
| Reactant | 1-Methylphenylphosphanium carbonate | HCID 86743659 | — |
| Solvent | Water | HCID 962 | — |
| Product | Phenylphosphine | HCID 12519 | — |
| Product | Methylphosphanium perchlorate | HCID 19871530 | — |
Reaction Steps
By following the same procedure as the 2nd step of Example 12 except that 10.0 g of 1-methylphenylphosphanium carbonate, 6.9 g of 60% perchlorate, and 10.0 g of water were used, 10.9 g (94.8% of the theoretical yield, yield of 67.6% to 1-phenylphosphane) of methylphosphanium perchlorate was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04892944 |
| Source dataset | uspto-grants-1990_01 |
| ORD ID | ord-f1dfed6d36574850a6245e0f377c767f |
| Source note | uspto-grants-1990_01 |