Maleic Anhydride → HCID 70360430, compound

HRID 329831Notes

Reaction equation

HRID 329831 reaction equation
CO[C:3](=[O:5])[O-:4].[CH3:6][N+:7]1([CH3:12])[CH2:11][CH2:10][CH2:9][CH2:8]1.C1(=O)[O:18][C:16](=[O:17])[CH:15]=[CH:14]1>O>[C:3]([O-:4])(=[O:5])/[CH:14]=[CH:15]\[C:16]([O-:18])=[O:17].[CH3:6][N+:7]1([CH3:12])[CH2:11][CH2:10][CH2:9][CH2:8]1.[CH3:6][N+:7]1([CH3:12])[CH2:11][CH2:10][CH2:9][CH2:8]1

Participants

4

Reactant 2

HCID 7923Maleic AnhydrideHCID 19871553HCID 19871553, compound

Product 1

HCID 70360430HCID 70360430, compoundYield 136.3%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

By following the same procedure as Example 20 (2nd step) except that 17.5 g of N,N-dimethylpyrrolidinium methyl carbonate, 17.5 g of water, and 9.8 g of maleic anhydride were used, 21.4 g (yield of 99.6%) of N,N-dimethylpyrrolidinium maleate was obtained. The content of mono-maleate was less than 0.1% and the contents of impurity ions were less than 1 ppm.

Sources & evidence

ORD record
ord-d681c7bf2b03478597cd74a1dc321a5f
Source dataset
uspto-grants-1990_01
Patent number
US04892944

Reaction notes

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