Maleic Anhydride → HCID 70360412, compound

HRID 329835Notes

Reaction equation

HRID 329835 reaction equation
CO[C:3](=[O:5])[O-:4].[CH3:6][N+:7]1([CH3:13])[CH2:12][CH2:11][CH2:10][CH2:9][CH2:8]1.C1(=O)[O:19][C:17](=[O:18])[CH:16]=[CH:15]1>O>[C:3]([O-:4])(=[O:5])/[CH:15]=[CH:16]\[C:17]([O-:19])=[O:18].[CH3:6][N+:7]1([CH3:13])[CH2:12][CH2:11][CH2:10][CH2:9][CH2:8]1.[CH3:6][N+:7]1([CH3:13])[CH2:12][CH2:11][CH2:10][CH2:9][CH2:8]1

Participants

4

Reactant 2

HCID 7923Maleic AnhydrideHCID 19871519HCID 19871519, compound

Product 1

HCID 70360412HCID 70360412, compoundYield 133.9%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

By following the same procedure as Example 20 (2nd step) except that 18.9 g of N,N-dimethylpiperidinium methyl carbonate, 18.9 g of water, and 9.8 g of maleic anhydride were used, 22.9 g (yield of 100%) of N,N-dimethylpiperidinium maleate was obtained. The content of monomethyl maleate was less than 0.1% and the content of impurity ions were all less than 1 ppm.

Sources & evidence

ORD record
ord-14f46d34d90f47e48f23a9b7a862b8ed
Source dataset
uspto-grants-1990_01
Patent number
US04892944

Reaction notes

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