HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 19870276, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 5-Chloro-1-pentanol | HCID 78915 | — |
| Reactant | HCID 19764216 | HCID 19764216 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 19870276 | HCID 19870276 | — |
Reaction Steps
20.0 grams (0.1 mole) 2-octylmorpholine, 13 grams (0.1 mole) of 5-chloropentanol and 12 grams of triethylamine in 150 ml. toluene were kept at 140°-150° C. for 12 hours in an autoclave. After cooling, the organic phase was washed twice with water, dried, and the solvent was evaporated and the base distilled at 128° C./0.01 mm Hg.; yield: 22.0 grams (77%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04894221 |
| Source dataset | uspto-grants-1990_01 |
| ORD ID | ord-52ff19e4caef4c2da5d591a4ea763b42 |
| Source note | uspto-grants-1990_01 |