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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 329986Erstellt: 25. Oktober 2026

Pyridine → 1-(2-Hexyl-4-tetradecylphenoxy)-3-(triphenylmethoxy)-2-propanol

https://huagongshe.com/reaction/329986

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPyridineHCID 1049—
EduktTrityl chlorideHCID 6456—
Edukt3-(2-Hexyl-4-tetradecylphenoxy)-1,2-propanediolHCID 14819670—
LösungsmittelChloroformHCID 6212—
Produkt1-(2-Hexyl-4-tetradecylphenoxy)-3-(triphenylmethoxy)-2-propanolHCID 1503026781,4%

Reaktionsschritte

A mixture of 11.64 g of 3-(2-hexyl-4-tetradecylphenoxy)-1,2-propanediol, 12.32 g of trityl chloride and 40 ml of pyridine was stirred for 24 hours, then diluted with chloroform, washed with aqueous sodium bicarbonate, water, dried and the solvents evaporated under reduced pressure. The residue was coevaporated with toluene, giving 14.6 g of the desired compound.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04894367
Quelldatensatzuspto-grants-1990_01
ORD IDord-da58882123674abc8b7bdf19bf7112ce
Quellennotizuspto-grants-1990_01