HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 14098085, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Methyl 4-sulfanylbenzoate | HCID 237573 | — |
| Reactant | HCID 15055905 | HCID 15055905 | — |
| Product | HCID 14098085 | HCID 14098085 | — |
Reaction Steps
8.3 ml of trifluoroacetic acid were added, whilst ice-cooling, to a mixture of 578 mg of methyl 4-mercaptobenzoate and 500 mg of 1-[2-hydroxy-2-(2-methoxyphenyl)ethyl]imidazole, and the mixture was stirred at a temperature between 0° and 5° C. for 2.7 hours, and then at room temperature for 2.5 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04894385 |
| Source dataset | uspto-grants-1990_01 |
| ORD ID | ord-cd15e0a5aca449108bf7c35b9ab30f4c |
| Source note | uspto-grants-1990_01 |