HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → Methyl 5-oxocyclopent-1-ene-1-heptanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | 9-Keto-12-oxo-dodecanoic acid, methyl ester | HCID 15093801 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Methyl 5-oxocyclopent-1-ene-1-heptanoate | HCID 2777884 | — |
Reaction Steps
A solution of the ester (VI) (10 g, 0.041 mole) in methanol (15 ml) is added dropwise, under nitrogen and stirring at reflux, to a solution of sodium methoxide [prepared from sodium (2.17 g; 0.094 mole) and methanol (280 ml)] At the end of the addition, the mixture is refluxed for 15 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04894473 |
| Source dataset | uspto-grants-1990_01 |
| ORD ID | ord-4c8f1a7c3ee24c60b4d3bf5113f6a201 |
| Source note | uspto-grants-1990_01 |