HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenylprop-2-Enal → HCID 346108, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenylprop-2-Enal | HCID 307 | — |
| Reactant | Benzoylhydrazine | HCID 11955 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 346108 | HCID 346108 | 88% |
Reaction Steps
To 200 ml of methanol solution containing 13.2 g of cinnamaldehyde was added 13.6 g of benzoylhydrazine, followed by stirring for 30 minutes at room temperature, for the precipitation of crystals. The crystals were filtered off and dried. Thus there was obtained 22 g of cinnamaldehyde benzoyl hydrazone (mp. 192°-194° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04895947 |
| Source dataset | uspto-grants-1990_01 |
| ORD ID | ord-e79f7a0de29b4c88b50afa4aa0c8a206 |
| Source note | uspto-grants-1990_01 |