Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → HCID 178444542, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | HCID 178444557 | HCID 178444557 | — |
| 생성물 | HCID 178444542 | HCID 178444542 | — |
반응 단계
A solution of 5 g of para-n-pentyl-transcyclohexanoic acid is refluxed in 8 ml of thionyl chloride for 2 hours. The thionyl chloride is then eliminated by distilling under atmospheric pressure. The acid chloride is then distilled under reduced pressure and under a dry nitrogen stream. This gives a product with a boiling point of 87° C. under 0.5 mm Hg.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04895986 |
| 출처 데이터셋 | uspto-grants-1990_01 |
| ORD ID | ord-39432e68030547ce8aaf09a224d625bb |
| 출처 메모 | uspto-grants-1990_01 |