HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-Hexylbenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-Hexylbenzoic acid | HCID 30725 | — |
| Product | 4-Hexylbenzoyl chloride | HCID 170863 | — |
Reaction Steps
A solution of 3 g of para-n-hexyl benzoic acid is refluxed in 7 ml of thionyl chloride for 2 hours. The thionyl chloride is eliminated by distillation under atmospheric pressure, followed by the distillation of the acid chloride under reduced pressure and under a dry nitrogen stream. This gives a product with a boiling point of 153° C. under 1.2 mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04895986 |
| Source dataset | uspto-grants-1990_01 |
| ORD ID | ord-802e8dc84fec484d923d32ad6ece63d2 |
| Source note | uspto-grants-1990_01 |