3,5-Di-tert-butyl-4-hydroxybenzoic acid → HCID 14674488, compound

HRID 330482Notes

Reaction equation

HRID 330482 reaction equation
[OH:1][C:2]1[C:10]([C:11]([CH3:14])([CH3:13])[CH3:12])=[CH:9][C:5]([C:6](O)=[O:7])=[CH:4][C:3]=1[C:15]([CH3:18])([CH3:17])[CH3:16].[NH2:19][C:20]1[CH:25]=[C:24]([N+:26]([O-])=O)[CH:23]=[CH:22][C:21]=1[OH:29]>>[NH2:26][C:24]1[CH:23]=[CH:22][C:21]([OH:29])=[C:20]([NH:19][C:6](=[O:7])[C:5]2[CH:4]=[C:3]([C:15]([CH3:16])([CH3:18])[CH3:17])[C:2]([OH:1])=[C:10]([C:11]([CH3:12])([CH3:14])[CH3:13])[CH:9]=2)[CH:25]=1

Participants

3

Reactant 2

HCID 150073,5-Di-tert-butyl-4-hydroxybenzoic acidHCID 36133892-Amino-4-Nitrophenol

Product 1

HCID 14674488HCID 14674488, compound

Procedure

4-hydroxy-3,5-di(tert.-butyl)benzoic acid and 2-amino-4-nitrophenol are treated in the same manner as described in Preparation 5-(1) and Preparation 1-(2) to give N-(5-amino-2-hydroxyphenyl)-4-hydroxy-3,5-di(tert.-butyl)benzamide are obtained.

Workup

  1. customas described in Preparation 5-(1) and Preparation 1-(2)

Sources & evidence

ORD record
ord-f2571c93014a4ebaa3af827bd2b60e18
Source dataset
uspto-grants-1990_01
Patent number
US04897393

Reaction notes

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