HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15114692, compound → HCID 14696444, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15114692 | HCID 15114692 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14696444 | HCID 14696444 | 100% |
Reaction Steps
A suspension of ethyl 5-nitro-2-naphthoate (8.0 g, 0.0326 mol) in EtOH (200 mL) was hydrogenated over 10% Pd/C (600 mg) at 50 psi for 3 hours 30 minutes. The mixture was filtered through Solka floc and concentrated to give a yellow solid (7.0 g, 100%), m.p. 94°-95° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04897405 |
| Source dataset | uspto-grants-1990_01 |
| ORD ID | ord-c46f5512c13d4c7fb8a6dcb83e6723ff |
| Source note | uspto-grants-1990_01 |