HRID330687

反应详情

EQUATION

反应方程式

HRID 330687 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a solution of 2.2 g (4.0 mmol) 3,3-bis(4-fluorophenyl)-2-[2-(triphenylmethyl)-2H-tetrazol-5-yl]-2-propenol in 100 mL methylene chloride was added 7 g of activated manganese dioxide. After stirring the resultant mixture for 20 hours, the insolubles were removed by filtration and the filtrate concentrated in vacuo to give a quantative yield of the title compound; m.p.=208° C. (dec).

WORKUP

后处理

  1. customthe insolubles were removed by filtration
  2. concentrationthe filtrate concentrated in vacuo