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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 330724Generated: October 25, 2026

Butyl isocyanate → Isopropyl butylcarbamate

https://huagongshe.com/reaction/330724

Reaction equation

Participants

RoleNameHCIDCharge
ReactantButyl isocyanateHCID 8110—
ReactantN,N',N''-Tris(3-dimethylaminopropyl)hexahydro-S-triazineHCID 85160—
ReactantIsocyanateHCID 105034—
SolventIsopropanolHCID 3776—
ProductIsopropyl butylcarbamateHCID 240398—

Reaction Conditions

Temperature60 °C

Reaction Steps

In a 250 ml round-bottomed flask, 0.02 g of Desmorapid Z, 31.1 g of n-butyl isocyanate were initially introduced and heated to 60° C. Thereafter, 18.9 g of isopropanol were added dropwise and the mixture was further kept at 60° C. until the isocyanate content had fallen below 0.1%. Thereafter, cooling was effected and the product was obtained as a clear liquid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08877408B2
Source datasetuspto-grants-2014_11
ORD IDord-dd72aa198be14ac5966dd35f8a2286f6
Source noteuspto-grants-2014_11