HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → Phenyl 3-(o-tolyl)propanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | 3-(2-Methylphenyl)propanoyl chloride | HCID 13029201 | — |
| Product | Phenyl 3-(o-tolyl)propanoate | HCID 86715420 | 93% |
Reaction Steps
The procedure as described in Example 4a) was repeated with phenol (48 mmol) and 3-o-tolylpropanoyl chloride (55 mmol). The crude product (12.4 g, 97%) was short path distilled at 127-129° C./0.05 mbar to yield 10.6 g (93%) of product as a colourless, semicrystalline oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08877704B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-653a29921ad541cd957e9893431a59c5 |
| Source note | uspto-grants-2014_11 |